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CH 328 Analytical Chemistry
Claycomb, Gregory D.


Mission Statement: Park University provides access to a quality higher education experience that prepares a diverse community of learners to think critically, communicate effectively, demonstrate a global perspective and engage in lifelong learning and service to others.

Vision Statement: Park University, a pioneering institution of higher learning since 1875, will provide leadership in quality, innovative education for a diversity of learners who will excel in their professional and personal service to the global community.

Course

CH 328 Analytical Chemistry Laboratory

Semester

FA 2012 HO

Faculty

Claycomb, Gregory D.

Title

Assistant Professor of Chemistry and Physics

Degrees/Certificates

B.S. Chemistry/University of New Mexico
Ph.D. Chemistry/Kansas State University

Office Location

Science 305

Office Hours

MW 1:00 - 2:00; TR 10:00 - noon

Daytime Phone

816-584-6338

E-Mail

gclaycomb@park.edu

Semester Dates

August 20th - December 14th

Class Days

T

Class Time

2:25 - 5:15 PM

Prerequisites

CH 108 and CH 108L

Credit Hours

4


Textbook:

All laboratory materials will be provided.

Textbooks can be purchased through the MBS bookstore

Textbooks can be purchased through the Parkville Bookstore

Additional Resources:

McAfee Memorial Library - Online information, links, electronic databases and the Online catalog. Contact the library for further assistance via email or at 800-270-4347.
Career Counseling - The Career Development Center (CDC) provides services for all stages of career development.  The mission of the CDC is to provide the career planning tools to ensure a lifetime of career success.
Park Helpdesk - If you have forgotten your OPEN ID or Password, or need assistance with your PirateMail account, please email helpdesk@park.edu or call 800-927-3024
Resources for Current Students - A great place to look for all kinds of information http://www.park.edu/Current/.


Course Description:
CH328 Analytical Chemistry: An in-depth study of classical analytical chemistry techniques. Subjects include the statistical evaluation of data, gravimetric and titrimetric methods of analysis, acid-base chemistry, complexation chemistry and redox processes. Laboratory includes practical examples of the methods covered in lecture. Prerequisites: CH108, CH108L. 3:4:4

Educational Philosophy:
The instructor's educational philosophy is one of interactiveness based on lectures, reading assignments, homework problem, quizzes and examinations, along with the laboratory techniques and principles.  The instructor will engage each learner to encourage the lively exploration of ideas and issues relevant to the modern aspects faced by analytical chemists.

Learning Outcomes:
  Core Learning Outcomes

  1. Compare and apply the theories upon which the principles of the various common analytical procedures are based.
  2. Examine and practice the important details of specific methods of analysis.
  3. Critically judge the accuracy and precision of experimental data by developing the necessary mathematical tools.
  4. Solve equilibrium and stoichiometric problems using proper techniques.
  5. Demonstrate the skill, competence, and confidence in the use of standard analytical laboratory equipment, including the proper use of a lab notebook, such that high quality analytical data can be obtained.


Core Assessment:
Lab technique, notebooks, written reports, lectures, quizzes, exams, review papers, homework.

Link to Class Rubric

Class Assessment:

Laboratory performance will be assessed upon laboratory reports.
 
The content of a laboratory report and the proper technique of keeping a laboratory notebook will be presented in class. 
 

Grading:
The laboratory scores will contribute 25% of the overall course grade. 

                               

Late Submission of Course Materials:
The instructor will not accept late assignments.

Classroom Rules of Conduct:

Cell phones must be turned off during class.

Course Topic/Dates/Assignments:

The laboratory schedule will be announced during class.

Academic Honesty:
Academic integrity is the foundation of the academic community. Because each student has the primary responsibility for being academically honest, students are advised to read and understand all sections of this policy relating to standards of conduct and academic life. Park University students and faculty members are encouraged to take advantage of the University resources available for learning about academic honesty (www.park.edu/current or http://www.park.edu/faculty/).from Park University 2011-2012 Undergraduate Catalog Page 95-96

Plagiarism:
Plagiarism involves the use of quotations without quotation marks, the use of quotations without indication of the source, the use of another's idea without acknowledging the source, the submission of a paper, laboratory report, project, or class assignment (any portion of such) prepared by another person, or incorrect paraphrasing. from Park University 2011-2012 Undergraduate Catalog Page 95

Attendance Policy:
Instructors are required to maintain attendance records and to report absences via the online attendance reporting system.

  1. The instructor may excuse absences for valid reasons, but missed work must be made up within the semester/term of enrollment.
  2. Work missed through unexcused absences must also be made up within the semester/term of enrollment, but unexcused absences may carry further penalties.
  3. In the event of two consecutive weeks of unexcused absences in a semester/term of enrollment, the student will be administratively withdrawn, resulting in a grade of "F".
  4. A "Contract for Incomplete" will not be issued to a student who has unexcused or excessive absences recorded for a course.
  5. Students receiving Military Tuition Assistance or Veterans Administration educational benefits must not exceed three unexcused absences in the semester/term of enrollment. Excessive absences will be reported to the appropriate agency and may result in a monetary penalty to the student.
  6. Report of a "F" grade (attendance or academic) resulting from excessive absence for those students who are receiving financial assistance from agencies not mentioned in item 5 above will be reported to the appropriate agency.

Park University 2011-2012 Undergraduate Catalog Page 98

Disability Guidelines:
Park University is committed to meeting the needs of all students that meet the criteria for special assistance. These guidelines are designed to supply directions to students concerning the information necessary to accomplish this goal. It is Park University's policy to comply fully with federal and state law, including Section 504 of the Rehabilitation Act of 1973 and the Americans with Disabilities Act of 1990, regarding students with disabilities. In the case of any inconsistency between these guidelines and federal and/or state law, the provisions of the law will apply. Additional information concerning Park University's policies and procedures related to disability can be found on the Park University web page: http://www.park.edu/disability .



Rubric

CompetencyExceeds Expectation (3)Meets Expectation (2)Does Not Meet Expectation (1)No Evidence (0)
Evaluation                                                                                                                                                                                                                                                 
Outcomes
1,2,4,5                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                              
-Assess a problem in analytical chemistry to determine what information is known/unknown and relevant/extraneous  -Evaluate a compound to determine   -state of compound  -appropriate procedure for analysis:  gravimetric, titrimetric, acid-base, complexation or redox   -Determine the percent composition to a reported value deviation of ? 1.0 % -Assess a problem in analytical chemistry to determine what information is known/unknown and relevant.  -Evaluate a compound to determine   -state of compound

-appropriate procedure for analysis:  gravimetric, titrimetric, or acid-base  -Determine the percent composition to a reported value deviation between 1.0-2.0%

 
-Assess a problem in analytical chemistry to determine what information is known and unknown.  -Evaluate a compound to determine  -state of compound  -appropriate procedure for analysis:  gravimetric or titrimetric

 -Determine the percent composition to a reported value deviation between 2.0-4.0%

 
-Assess a problem in analytical chemistry to determine what information is known.  -Evaluate a compound to determine  -state of compound  -appropriate titrimetric procedure for analysis  -Determine the percent composition to a reported value deviation between > 4.0%



 
Synthesis                                                                                                                                                                                                                                                  
Outcomes
1,2,4,5,7                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                            
-Propose an appropriate procedure to evaluate the percent composition of a sample.  -Show a proficiency in the laboratory in each of the following:  -statistical evaluation of data, gravimetric, titrimetric, acid-base, complexation and redox methods of analysis  -Keep a well organized, legible laboratory notebook that can be used for a patent project or for legal purposes.  All ideas, inventions, procedures, experimentation records, observations and all work in detail must be recorded.  (Procedure, data, results, discussion, and conclusion can be understood by an outsider.) -Select from an extensive list the appropriate procedure to evaluate the percent composition of a sample.  -Show a proficiency in the laboratory  in five of the following:  statistical evaluation of data, gravimetric, titrimetric, acid-base, complexation and redox methods of analysis  -Keep a well organized, legible laboratory notebook that can be used for a project.  All ideas, procedures, experimentation records, observations and all work in detail must be recorded.  (Procedure, data, results, discussion, and conclusion can be understood by an outsider.) -Select from a list of five the appropriate procedure to evaluate the percent composition of a sample.  -Show a proficiency in the laboratory  in three or four of the following:  statistical evaluation of data, gravimetric, titrimetric, acid-base, complexation and redox methods of analysis  -Keep a well organized, legible laboratory notebook that can be used for a project.  All procedures, experimentation records and work in detail must be recorded.  (Procedure and data can be understood by an outsider.) -Select from a list of two the appropriate procedure to evaluate the percent composition of a sample.  -Show a proficiency in the laboratory  in two or less of the following:  statistical evaluation of data, gravimetric, titrimetric, acid-base, complexation and redox methods of analysis   -Calculate the average value of observables using a given wave function  -Keep a legible laboratory notebook.  All procedures and experimentation records must be recorded.  (Only the procedure can be understood by an outsider.) 
Analysis                                                                                                                                                                                                                                                   
Outcomes
1,2,3,4                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                              
-Analyze all but 2 samples of unknowns via the following methods:  gravimetric chloride and nickel, standardization of NaOH and KMnO4, %KHP determination, % soda ash, hardness of water with EDTA, % fluoride, %Fe by redox, and electrochemical deposition within 1.0% accuracy -Analyze all but 3 samples of unknowns via the following methods:  gravimetric chloride and nickel, standardization of NaOH and KMnO4, %KHP determination, % soda ash, hardness of water with EDTA, % fluoride, %Fe by redox, and electrochemical deposition between 1.0-2.0% accuracy -Analyze samples of 4 unknowns via the following methods:  gravimetric chloride and nickel, standardization of NaOH and KMnO4, %KHP determination, % soda ash, hardness of water with EDTA, % fluoride, %Fe by redox, and electrochemical deposition between 2.0-4.0% accuracy -Analyze all of 4samples of  unknowns via the following methods:  gravimetric chloride and nickel, standardization of NaOH and KMnO4, %KHP determination, % soda ash, hardness of water with EDTA, % fluoride, %Fe by redox, and electrochemical deposition between 4.0-5.0% accuracy 
Application                                                                                                                                                                                                                                                
Outcomes
1,2,4,5                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                              
-Apply gravimetric, titrimetric, redox, acid-base, complexation methods to analyze unknown compounds within 1.0% accuracy  -Demonstrate the use of an ion-selective electrode to determine the % composition of an unknown within 1.0% accuracy  -Statistically evaluate data -Apply gravimetric, titrimetric, redox, acid-base, complexation methods to analyze unknown compounds between 1.0-2.0% accuracy  -Demonstrate the use of an ion-selective electrode to determine the % composition of an unknown between 1.0-2.0% accuracy  -Statistically evaluate data -Apply gravimetric, titrimetric, redox, acid-base, complexation methods to analyze unknown compounds between 2.0-4.0% accuracy  -Demonstrate the use of an ion-selective electrode to determine the % composition of an unknown between between 2.0-4.0% accuracy -Apply gravimetric, titrimetric, redox, acid-base, complexation methods to analyze unknown compounds between 4.0-5.0% accuracy  -Demonstrate the use of an ion-selective electrode to determine the % composition of an unknown between between 4.0-5.0% accuracy 
Content of Communication                                                                                                                                                                                                                                   
Outcomes
1,2,4                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                
-Keep a high quality lab notebook

 -Illustrate a complete understanding of each lab by submitting a well organized, legible laboratory notebook that can be used for a patent project or for legal purposes.  All ideas, inventions, procedures, experimentation records, observations and all work in detail must be recorded.  (Procedure, data, results, discussion, and conclusion can be understood by an outsider.)

 -Illustrate complete understanding of lab questions by neatly and in an orderly manner present the solution showing equations, derivations, insertions, answers, and explaining all steps.

 
-Keep a quality lab notebook  -Illustrate a complete understanding of each lab by submitting a well organized, legible laboratory notebook that can be used for a project.  All ideas, procedures, experimentation records, observations and all work in detail must be recorded.  (Procedure, data, results, discussion, and conclusion can be understood by an outsider.)  -Illustrate complete understanding of lab questions by neatly and in an orderly manner present the solution showing equations, insertions, answers, and explaining all steps. -Keep a lab notebook  -Illustrate a complete understanding of each lab by submitting an organized, legible laboratory notebook that can be used for a project.  All procedures, experimentation records and work in detail must be recorded.  (Procedure and data can be understood by an outsider.)  -Illustrate complete understanding of lab questions by neatly and in an orderly manner present the solution showing equations, insertions, and answers. -Keep a lab notebook  -Illustrate a complete understanding of each lab by submitting an organized, legible laboratory notebook.  All procedures and experimentation records must be recorded.  (Only the procedure can be understood by an outsider.)  -Illustrate complete understanding of lab questions by neatly and in an orderly manner present the solution showing equations with insertions and answers. 
Technical Skill in Communicating                                                                                                                                                                                                                           
Outcomes
2,4,5                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                
-Manipulate data following the principles of common analytical procedures  -Create spread sheets to evaluate data  -Graph data  -Interpret graphical representation of data  -Judge the accuracy and precision of data by developing the necessary mathematical tools of the laboratory -Manipulate data following the principles of common analytical procedures  -Create spread sheets to evaluate data  -Graph data  -Interpret graphical representation of data  -Judge the accuracy and precision of data by using given statistical procedures of the laboratory -Manipulate data following the principles of common analytical procedures making minor errors  -Create spread sheets to evaluate data  -Graph data  -Interpret graphical representation of data -Manipulate data following the principles of common analytical procedures making major and minor errors  -Create spread sheets to evaluate data  -Graph data



 
Nomenclature and Periodicity                                                                                                                                                                                                                               
Outcomes
1,2,3                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                
-Demonstrate a knowledge of inorganic and organic nomenclature  -Demonstrate a complete knowledge of the periodic table -Demonstrate a knowledge of inorganic nomenclature (nonmetals and metals)  -Demonstrate a knowledge of periodic trends -Demonstrate a knowledge of inorganic nomenclature (metals)  -Demonstrate a knowledge of two periodic trends -Demonstrate a knowledge of atomic names.  -Demonstrate a knowledge of one periodic trend 
Solutions                                                                                                                                                                                                                                                  
Outcomes
1,2                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                  
Demonstrate the ability to make and dilute solutions quantitatively and perform the necessary calculations for any concentration Demonstrate the ability to make and dilute solutions quantitatively and perform the necessary calculations for molarity, molality, and normality Demonstrate the ability to make and dilute solutions quantitatively and perform the necessary calculations for molarity Demonstrate the ability to make and dilute solutions 

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Last Updated:8/17/2012 4:46:39 PM