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CH 429 Advanced Analytical Chemistry
Claycomb, Gregory D.


Mission Statement: Park University provides access to a quality higher education experience that prepares a diverse community of learners to think critically, communicate effectively, demonstrate a global perspective and engage in lifelong learning and service to others.

Vision Statement: Park University, a pioneering institution of higher learning since 1875, will provide leadership in quality, innovative education for a diversity of learners who will excel in their professional and personal service to the global community.

Course

CH 429 Advanced Analytical Chemistry

Semester

SP 2013 HOZ

Faculty

Claycomb, Gregory D.

Degrees/Certificates

Ph.D. Kansas State University

Office Location

SC 305

Office Hours

Monday -  Friday 9:00 - 11:00

Daytime Phone

816-584-6338

E-Mail

gclaycomb@park.edu

Class Days

M-W-F

Class Time

M W 11:00-11:50 lecture; W F 1:30-4:20 laboratory

Prerequisites

permission of instructor

Credit Hours

4


Textbook:
Course materials will be provided in class.

Additional Resources:

McAfee Memorial Library - Online information, links, electronic databases and the Online catalog. Contact the library for further assistance via email or at 800-270-4347.
Career Counseling - The Career Development Center (CDC) provides services for all stages of career development.  The mission of the CDC is to provide the career planning tools to ensure a lifetime of career success.
Park Helpdesk - If you have forgotten your OPEN ID or Password, or need assistance with your PirateMail account, please email helpdesk@park.edu or call 800-927-3024
Resources for Current Students - A great place to look for all kinds of information http://www.park.edu/Current/.


Course Description:
CH429 Advanced Analytical Chemistry: Advanced methods of chemical analysis stressing, but not limited to, instrumental techniques. An in-depth study of the theory of electrochemical measurements, spectroscopic techniques, and chromatographic theory will be covered. Students will be introduced to several modern techniques including Raman, X-ray, and flame and furnace atomic absorption spectroscopy, thermal methods of analysis and NMR techniques. Some applications of advanced methods of classical analysis will be covered. Prerequisites: CH318, CH329. 3:4:4

Educational Philosophy:
The instructor's educational philosophy is based upon student engagement with lecture material, reading assignments, homework problems, quizzes and examinations, along with the laboratory techniques and principles.  The instructor will encourage each student to explore the of ideas and issues relevant to the modern aspects faced by analytical chemists.

Learning Outcomes:
  Core Learning Outcomes

  1. Describe, explain, and apply various spectroscopic techniques.
  2. Demonstrate proficiency in working the flame and furnace atomic absorption spectrophotometers and the Inductively Couple Plasma (ICP) Spectrometry and its applications at Park University
  3. Demonstrate proficiency in the dual column GC and GC/MS, SCF extractor, HPLC, and NMR.
  4. Select the proper technique and design the procedure for a specific analysis.


Core Assessment:

Link to Class Rubric

Class Assessment:
The primary course assessment will be written laboratory reports.

Grading:
There will be six lab reports, each worth 100 points.

Course Topic/Dates/Assignments:
Assignments will be announced in class.

Academic Honesty:
Academic integrity is the foundation of the academic community. Because each student has the primary responsibility for being academically honest, students are advised to read and understand all sections of this policy relating to standards of conduct and academic life. Park University students and faculty members are encouraged to take advantage of the University resources available for learning about academic honesty (www.park.edu/current or http://www.park.edu/faculty/).from Park University 2011-2012 Undergraduate Catalog Page 95-96

Plagiarism:
Plagiarism involves the use of quotations without quotation marks, the use of quotations without indication of the source, the use of another's idea without acknowledging the source, the submission of a paper, laboratory report, project, or class assignment (any portion of such) prepared by another person, or incorrect paraphrasing. from Park University 2011-2012 Undergraduate Catalog Page 95

Attendance Policy:
Instructors are required to maintain attendance records and to report absences via the online attendance reporting system.

  1. The instructor may excuse absences for valid reasons, but missed work must be made up within the semester/term of enrollment.
  2. Work missed through unexcused absences must also be made up within the semester/term of enrollment, but unexcused absences may carry further penalties.
  3. In the event of two consecutive weeks of unexcused absences in a semester/term of enrollment, the student will be administratively withdrawn, resulting in a grade of "F".
  4. A "Contract for Incomplete" will not be issued to a student who has unexcused or excessive absences recorded for a course.
  5. Students receiving Military Tuition Assistance or Veterans Administration educational benefits must not exceed three unexcused absences in the semester/term of enrollment. Excessive absences will be reported to the appropriate agency and may result in a monetary penalty to the student.
  6. Report of a "F" grade (attendance or academic) resulting from excessive absence for those students who are receiving financial assistance from agencies not mentioned in item 5 above will be reported to the appropriate agency.

Park University 2011-2012 Undergraduate Catalog Page 98

Disability Guidelines:
Park University is committed to meeting the needs of all students that meet the criteria for special assistance. These guidelines are designed to supply directions to students concerning the information necessary to accomplish this goal. It is Park University's policy to comply fully with federal and state law, including Section 504 of the Rehabilitation Act of 1973 and the Americans with Disabilities Act of 1990, regarding students with disabilities. In the case of any inconsistency between these guidelines and federal and/or state law, the provisions of the law will apply. Additional information concerning Park University's policies and procedures related to disability can be found on the Park University web page: http://www.park.edu/disability .



Rubric

CompetencyExceeds Expectation (3)Meets Expectation (2)Does Not Meet Expectation (1)No Evidence (0)
Evaluation                                                                                                                                                                                                                                                 
Outcomes
1,2,4                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                
• Using proper instrumentation evaluate the absorption or emission of light by a compound.  


• Demonstrate a knowledge and understanding of radiation detectors and the appropriate electronics.


• Completely interpret complex NMR Spectra


• Demonstrate a knowledge and understanding of X-Ray spectroscopy and quantitative analysis.


• Completely interpret simple mass spectrophotometer output.


• For all experiments be able to design a reasonable procedure for a specific analysis.





 
• Using proper instrumentation (with two errors) evaluate the absorption or emission of light by a compound.  

• Demonstrate a knowledge and understanding of radiation detectors.

• Completely interpret simple NMR Spectra

• Demonstrate knowledge of X-Ray spectroscopy and indicate some applications.

• Completely interpret simple mass spectrophotometer output.

• For 85% of the experiments design a reasonable procedure for a specific analysis.



 
• Using proper instrumentation (with 4 errors) evaluate the absorption or emission of light by a compound.  

• Demonstrate knowledge of radiation detectors.

• Partially interpret simple NMR Spectra

• Demonstrate an elementary knowledge of X-Ray spectroscopy.

• Partially interpret simple mass spectrophotometer output.

• For 75% of the experiments design a reasonable procedure for a specific analysis.



 
• Using proper instrumentation evaluate the absorption or emission of light by a compound for two methods.  

• Knows the function of a detector.

• Generally cannot interpret simple NMR Spectra

• Demonstrate an elementary knowledge of an X-Ray spectroscopy.

• Generally cannot interpret simple mass spectrophotometer output.

• For 65% of the experiments design a reasonable procedure for a specific analysis.



 
Synthesis                                                                                                                                                                                                                                                  
Outcomes
1,2,4,5,7                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                            
• Demonstrate an understanding of the components in absorption, fluorescence, phosphorescence, scattering, emission, and Chemiluminescence by diagrams, sample outputs, and electronics.

• Demonstrate complete knowledge (includes electronics) of the common radiation sources, wavelength selectors, and performance characteristics of monochromators.

• Describe all the components of the following instruments:  AA, ICP, GC/MS, SFC, HPLC, MS, and NMR.

• Given an unknown, select the proper technique for all analyses.

• Demonstrate an understanding (including electronics) of the components in GC, HPLC, FTIR, and SCF.

• Demonstrate an understanding of the electronic operation of detectors and the way they transform chemical information.





 
• Demonstrate an understanding of the components in absorption, fluorescence, phosphorescence, scattering, emission, and Chemiluminescence by diagrams and sample output.

• Demonstrate knowledge of the common radiation sources, wavelength selectors, and performance characteristics of monochromators.

• Describe the major components of the following instruments:  AA, ICP, GC/MS, SFC, HPLC, MS, and NMR.

• Given an unknown, select the proper technique for 85% of analyses.

• Demonstrate an understanding of the components in GC, HPLC, FTIR, and SCF.

• Demonstrate an understanding of the operation of detectors and the way they transform chemical information.



 
• Demonstrate an understanding of the components in four of the following:  absorption, fluorescence, phosphorescence, scattering, emission, and Chemiluminescence by diagrams and sample output.

• Demonstrate elementary knowledge of the common radiation sources, wavelength selectors, and performance characteristics of monochromators.

• Describe the major components in five of the following instruments:  AA, ICP, GC/MS, SFC, HPLC, MS, and NMR.

• Given an unknown, select the proper technique for 75% of analyses.

• Demonstrate an understanding of the components in two of the following:  GC, HPLC, FTIR, and SCF.

• Demonstrate an elementary understanding of the operation of detectors.



 
• Demonstrate an understanding of the components in two of the following:  absorption, fluorescence, phosphorescence, scattering, emission, and Chemiluminescence by diagrams and sample output.

• Demonstrate elementary knowledge of the common radiation sources and wavelength selectors of monochromators.

• Describe the major components in three of the following instruments:  AA, ICP, GC/MS, SFC, HPLC, MS, and NMR.

• Given an unknown, select the proper technique for 65% of analyses.

• Demonstrate an understanding of the components in one of the following:  GC, HPLC, FTIR, and SCF.

• Can identify a detector.

 
Analysis                                                                                                                                                                                                                                                   
Outcomes
1,2,3,4                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                              
• Describe the Matrix effects and the use of internal standards and spiking during an analysis.

• Analyze the results form a MS, FTIR, UV-Vis, NMR, Fluorescence, phosphorescence, chemiluminescence, AA, Emission, Raman spectroscopy

• Determine the correct column for use in GC and use it for analysis.

• Determine the correct method for HPLC analysis.  



 
• Describe the use of internal standards and spiking during an analysis.

• Analyze the results form eight of the following:  MS, FTIR, UV-Vis, NMR, Fluorescence, phosphorescence, chemiluminescence, AA, Emission, Raman spectroscopy

• Determine a set of columns for use in GC and use one for analysis.

• Determine the correct method with minor errors for HPLC.



 
• Describe the use of internal standards or spiking during an analysis.

• Analyze the results form six of the following:  MS, FTIR, UV-Vis, NMR, Fluorescence, phosphorescence, chemiluminescence, AA, Emission, Raman spectroscopy

• Given a list of four columns for use in GC, select the correct one and use it for analysis.

• Determine the correct method with minor errors for HPLC analysi.

 
• Does not know the purpose of the addition of known compounds to samples before analysis.

• Analyze the results form five of the following:  MS, FTIR, UV-Vis, NMR, Fluorescence, phosphorescence, chemiluminescence, AA, Emission, Raman spectroscopy

• Given a list of two columns for use in GC, select the correct one and use it for analysis.

• List the basic procedure for aHPLC run.

 
Application                                                                                                                                                                                                                                                
Outcomes
1,2,4,5                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                              
• Apply Molecular UV-Vis Absorption Spectroscopy and interpret the results.

• Apply Molecular Fluorescence, Phosphorescence, and Chemiluminescence.

• Apply AA Spectroscopy and determine the concentration varying techniques (matrix, spiked, internal standard).

• Describe an application of Emission Spectroscopy based upon Plasma, Arc, and Spark Atomization.

• Apply IR, FTIR, NIR, and Raman spectroscopy

• Demonstrate a complete understanding of a mass spectrometer.  

• Apply GC and HPLC to a sample and know when to each method.  

 
• Apply Molecular UV-Vis Absorption Spectroscopy and obtain the spectra with little interpretation.

• Apply AA Spectroscopy and determine the concentration using an internal standard or spiked sample.

• Describe an application of Emission Spectroscopy based upon Plasma, Arc, and Spark Atomization.

• Apply IR, FTIR, and NIR spectroscopy

• Demonstrate a partial understanding of a mass spectrometer.  

• Apply GC and HPLC to a sample.  

 
• Apply Molecular UV-Vis Absorption Spectroscopy and obtain a spectrum.

• Apply AA Spectroscopy to an unaltered sample.

• Describe an application of Emission Spectroscopy based upon Plasma, Arc, or Spark Atomization.

• Apply FTIR spectroscopy

• Diagram the major components of a MS.

• Apply GC or HPLC to a sample.  

 
• Can Diagram a Spec. 20 Spectrophotometer.

• Can calibrate the instrument...

• Describe elementary Emission Spectroscopy.

• Describe an IR.

• Describe a Mass Spectrophotometer and what it does.

• Describe basic chromatography.  

 
Content of Communication                                                                                                                                                                                                                                   
Outcomes
1,2,4                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                
• Illustrate a complete understanding of all instruments by answering all questions on each correctly.

• Illustrate complete understanding of questions by neatly and in an orderly manner presenting the solution showing equations, derivations, insertions, answers, and explaining all steps.

 
• Illustrate a complete understanding of all instruments by answering all questions on each 90% correctly.

• Illustrate complete understanding of questions by neatly and in an orderly manner presenting the solution showing equations, insertions, answers, and explaining all steps.

 
• Illustrate a complete understanding of  all instruments by answering all questions on each 80% correctly.

• Illustrate complete understanding of questions by neatly and in an orderly manner presenting the solution showing equations, insertions, and answers.

 
• Illustrate a complete understanding of  all instruments by answering all questions on each 70% correctly.

• Illustrate some understanding of questions by neatly and in an orderly manner presenting the solution showing insertions, and answers.

 
Technical Skill in Communicating                                                                                                                                                                                                                           
Outcomes
2,4,5                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                
• Manipulate data following the principles of common analytical procedures

• Create spread sheets to evaluate data

• Graph data

• Interpret graphical representation of data

• Demonstrate the ability to sample and interpret the results for AA, UV-Vis, GC, HPLC, FTIR, ICP

 
• Manipulate data following the principles of common analytical procedures

• Create spread sheets to evaluate data

• Graph data

• Interpret graphical representation of data

• Demonstrate the ability to sample and interpret the results for  five of the following:  AA, UV-Vis, GC, HPLC, FTIR, ICP

 
• Manipulate data following the principles of common analytical procedures making minor errors

• Create spread sheets to evaluate data

• Graph data

• Interpret graphical representation of data

• Demonstrate the ability to sample and interpret the results for  four of the following:  AA, UV-Vis, GC, HPLC, FTIR, ICP

 
• Manipulate data following the principles of common analytical procedures making major and minor errors

• Create spread sheets to evaluate data

• Graph data

• Demonstrate the ability to sample and interpret the results for three of the following:  AA, UV-Vis, GC, HPLC, FTIR, ICP



 
Nomenclature and Periodicity                                                                                                                                                                                                                               
Outcomes
1,3,5                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                
• Demonstrate a knowledge of inorganic and organic nomenclature



• Demonstrate a complete knowledge of the periodic table



 
• Demonstrate a knowledge of inorganic nomenclature (nonmetals and metals)

• Demonstrate a knowledge of periodic trends

 
• Demonstrate a knowledge of inorganic nomenclature (metals)



• Demonstrate a knowledge of two periodic trends

 
• Demonstrate knowledge of atomic names.



• Demonstrate a knowledge of one periodic trend

 
Solutions                                                                                                                                                                                                                                                  
Outcomes
1,2                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                  
Demonstrate the ability to make and dilute solutions quantitatively and perform the necessary calculations for any concentration Demonstrate the ability to make and dilute solutions quantitatively and perform the necessary calculations for molarity, molality, and normality Demonstrate the ability to make and dilute solutions quantitatively and perform the necessary calculations for molarity Demonstrate the ability to make and dilute solutions 

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Last Updated:1/11/2013 2:00:34 PM